河南师范大学化学与环境科学学院黄淮水环境与污染防治省部共建教育部重点实验室
纸质出版:2011
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[1]王晓兵,李培,娄向东,赵晓华,王学锋.铁掺杂In_2O_3纳米粉体及其气敏性能研究[J].传感器与微系统,2011,30(01):13-15.
WANG Xiao-bing, LI Pei, LOU Xiang-dong, et al. Research on Fe doped In2O3 nano-powder and its gas sensitive properties[J]. 2011, 30(1): 13-15.
[1]王晓兵,李培,娄向东,赵晓华,王学锋.铁掺杂In_2O_3纳米粉体及其气敏性能研究[J].传感器与微系统,2011,30(01):13-15. DOI: 10.13873/j.1000-97872011.01.002.
WANG Xiao-bing, LI Pei, LOU Xiang-dong, et al. Research on Fe doped In2O3 nano-powder and its gas sensitive properties[J]. 2011, 30(1): 13-15. DOI: 10.13873/j.1000-97872011.01.002.
对In2O3粉体进行Fe掺杂
采用水热法合成了In2O3粉体。通过X射线衍射(XRD)
扫描电镜(SEM)
透射电子显微镜(TEM)等手段对粉体的物相、形貌、粒度等进行表征。TEM图表明:质量分数为7%Fe掺杂的样品为均匀排列的棒
长度约为300~500 nm
宽度约20 nm。对样品进行气敏性能研究
结果表明:质量分数为7%Fe掺杂的In2O3气敏元件
当工作温度为125℃时
对100×10-6Cl2的灵敏度高达182.75。元件对10×10-6Cl2的灵敏度为17.9
可以检测到低体积分数的Cl2。并具有选择性好、响应-恢复时间短等特性。
The preparation of Fe doped In2O3 nano-powder using a hydrothermal method is introduced.Its size
phase and morphology are analyzed by XRD
SEM and TEM.The gas sensing characteristics of the materials are tested in static slate.The results show that the morphology of the In2O3 with mass fraction 7% Fe is rods with good dispersity.The average length of the as-synthesized rods is about 300~500nm
and the width is 20 nm.The In2O3 with mass fraction 7% Fe has the highest sensitivity as high as 182.75 to 100×10-6 Cl2 at lower working temperature 125℃.And the In2O3 with mass fraction 7% Fe also has a high sensitivity as high as 17.9 to 10×10-6 Cl2 at 125℃.So the sensors can tests low volume fraction of Cl2.The sensor based on In2O3 also has satisfied selectivity
quick response and recover.
表面活性剂-水热法一步制备纳米In 2 O 3 气敏材料 [J]. 娄向东,李培,王晓兵,秦楠,王学峰. 硅酸盐通报 . 2009(06)
水热法合成纯立方铁锰矿型In 2 O 3 晶体 [J]. 董国义,田帅,姚金宝,李哲,胡志鹏,韦志仁. 人工晶体学报 . 2008(06)
Al 2 O 3 -La 2 O 3 共掺杂对ZnO纳米粉体气敏性能的影响 [J]. 牛新书,王雪丽,李华,魏平涛,茹祥莉,陈晓丽. 传感器与微系统 . 2008(11)
氧化铟纳米材料的制备及其在气体传感器中的应用 [J]. 郭书玲,王晓华,徐甲强,王焕新. 传感器世界 . 2006(05)
In 2 O 3 基纳米氨敏传感器材料的制备、结构及气敏特性 [J]. 郭鹏峰,潘海波. 福州大学学报(自然科学版) . 2005(03)
氧化铟气敏材料的制备与特性 [J]. 刘秉涛,姜安玺,徐甲强. 稀有金属材料与工程 . 2004(10)
Low voltage cathodoluminescent properties of phosphors coated with In 2 O 3 by sol-gel method [J] . H. Kominami,T. Nakamura,K. Sowa,Y. Nakanishi,Y. Hatanaka,G. Shimaoka. Applied Surface Science . 1997
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