重庆师范大学物理与电子工程学院重庆市光电功能材料重点实验室
纸质出版:2023
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龚庭韦, 史笑岩, 谢远航, 等. 镉钯共掺ZnO的制备与H2气敏性能研究[J]. 传感器与微系统, 2023,(5):6-11.
龚庭韦, 史笑岩, 谢远航, 等. 镉钯共掺ZnO的制备与H2气敏性能研究[J]. 传感器与微系统, 2023,(5):6-11. DOI: 10.13873/J.1000-9787(2023)05-0006-06.
采用一步水热法制备了镉(Cd)、钯(Pd)共掺氧化锌(ZnO)纳米材料。通过X射线衍射(XRD)、扫描电镜(SEM)、拉曼光谱和光致发光(PL)光谱对制备的样品进行了表征与分析,并对其氢气(H
2
)气敏性能进行了系统测试分析。实验制得样品为六方纤锌矿晶体结构,具有良好的结晶度;Cd、Pd的掺入改善了ZnO的结构,调控晶体缺陷;基于Cd、Pd共掺ZnO基传感器的检测体积分数、响应恢复时间和工作温度都有明显降低;并且该材料在60℃低温下对H
2
仍具有良好的响应。最后,对Cd、Pd共掺ZnO的气敏原理也进行了探讨。
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